Shinwa Chemical Industries Ltd.
LC/GC Search / Application Note

Shinwa Chemical Industries
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"Ethyl Acetate" Filtered 41 Item.

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GC

Samples
Methyl Alcohol , Ethyl Alcohol , Isopropyl Alcohol , Ethyl Acetate , Methyl Ethyl Ketone , Benzene , Methyl Isobutyl Ketone , Toluene , Butyl Acetate , Cellosolve , Ethylbenzene , m-Xylene , p-Xylene , o-Xylene , Cyclohexanone
Applications
Organic solvents (2)
Column
SBS-1 10% Shimalite TPA 60-80
Column Size
3.1m×3.2mm
Column temp.
100°C
Carrier gas
N2,40ml/min
Injection port temp.
230°C
Detector temp.
230°C(FID)

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GC

Samples
n-Hexane , Methyl Alcohol , Acetone , Isopropyl Alcohol , Ethyl Acetate , Methyl Ethyl Ketone , Benzene , Trichloroethylene , Isobutyl Alcohol , Isobutyl Acetate , Toluene , n-Butyl Acetate , Isoamyl Alcohol , Ethylbenzene , m-Xylene , o-Xylene , n-Propylbenzene , Cyclohexanone
Applications
Organic solvent in the air (ppm level)
Column
SBS-100 10% Shimalite TPA 60-80
Column Size
3.1m×3.2mm
Column temp.
110°C
Carrier gas
N2,30ml/min
Injection port temp.
200°C
Detector temp.
200°C(FID)

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GC

Samples
Acetone , Isopropyl Alcohol , n-Hexane , Ethyl Acetate , Chloroform , Carbon Tetrachloride , n-Butyl Alcohol , Methyl Isobutyl Ketone , Isobutyl Acetate , Toluene , n-Butyl Acetate , Ethylbenzene , m-Xylene , o-Xylene , Cyclohexanone , Butyl Cellosolve , 1,1,2,2-Tetrachloroethane , o-Dichlorobenzene
Applications
Organic solvent in work environment (2)
Column
SBS-200 20% Shimalite W 100-120 (AW-DMCS)
Column Size
3.1m×3.2mm
Column temp.
100°C
Carrier gas
N2,50ml/min
Injection port temp.
240°C
Detector temp.
240°C(FID)

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GC

Samples
Acetone , Isopropyl Alcohol , n-Hexane , Ethyl Acetate , Chloroform , Carbon Tetrachloride , n-Butyl Alcohol , Methyl Isobutyl Ketone , Isobutyl Acetate , Toluene , n-Butyl Acetate , Ethylbenzene , m-Xylene , o-Xylene , Cyclohexanone , Butyl Cellosolve , 1,1,2,2-Tetrachloroethane , o-Dichlorobenzene
Applications
Organic solvents of the atmosphere (ppm level)
Column
SBS-200 20% Shimalite W 100-120 (AW-DMCS)
Column Size
3.1m×3.2mm
Column temp.
100°C
Carrier gas
N2,50ml/min
Injection port temp.
240°C
Detector temp.
240°C(FID)

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GC

Samples
Ethyl Acetate , Acetaldehyde-2,4-Dinitrophenylhydrazone
Applications
Acetaldehyde -2,4- dinitrophenylhydrazone
Column
Silicone OV-17 1% Chromosorb W 80-100 (AW-DMCS)
Column Size
2.1m×3.2mm
Column temp.
220°C
Carrier gas
N2,60ml/min
Injection port temp.
270°C
Detector temp.
270°C(FID)

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GC

Samples
Methanol , Acetaldehyde , Ethanol , Isopropanol , n-Propanol , Ethyl Acetate , Isobutanol , n-Butanol , Isoamyl Alcohol
Applications
Lower alcohol in water
Column
Thermon-1000 5% Sunpak-A
Column Size
2.1m×3.2mm
Column temp.
180°C
Carrier gas
N2,50ml/min
Injection port temp.
240°C
Detector temp.
240°C(FID)

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GC

Samples
α-Pinene , β-Pinene , Limonene , Octyl Aldehyde , Nonyl Aldehyde , Citronellal , Decyl Aldehyde , Linalool , Linalyl Acetate , Isobornyl Acetate(Citronellol) , Menthol , Benzyl Acetate , Perillaldehyde , Geraniol , α-Ionone , Rose-P , C12-Alcohol , Anisaldehyde , Methyl Cinnamate , Ethyl Cinnamate , Eugenol , Heliotropin , DEP , Vanillin , Benzyl Benzoate , Benzyl Salicylate
Applications
The mixed sample of perfume component
Column
Thermon-3000 5% Chromosorb W 80-100 (AW-DMCS)
Column Size
3.1m×3.2mm
Column temp.
80°C→250°C(6°C/min)
Carrier gas
N2,60ml/min
Injection port temp.
290°C
Detector temp.
280°C(FID)

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GC

Samples
Dimethyl Ether , Methanol , Isopropanol , Methyl Ethyl Ketone , Isopropyl Acetate , 2-Butanol , n-Propyl Acetate , Isobutanol , Dioxane , Methyl Cellosolve , Toluene , Ethyl Cellosolve , N,N-Dimethylformamide , Chlorobenzene , Cellosolve Acetate , Cyclohexanone , Cyclohexanol , 2-Methyl Cyclohexanone , 2-Methyl Cyclohexanol , o-Dichlorobenzene
Applications
Organic solvents (4)
Column
Ucon LB 550X 20% Chromosorb W 80-100 (AW)
Column Size
3.1m×3.2mm
Column temp.
100°C
Carrier gas
N2,50ml/min
Injection port temp.
230°C
Detector temp.
230°C(FID)

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GC

Samples
Solvents
Applications
Solvents (5)
Column
ULBON HR-1
Column Size
50m×0.25mm(0.5μm)
Column temp.
60°C→120°C(2°C/min)
Carrier gas
He,0.93ml/min
Detector temp.
150°C(FID)
Injection volume
1μl

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GC

Samples
Methanol , Ethyl Ether , Isopropanol , trans-1,2-Dichloroethylene , Ethyl Acetate , Chloroform , Isobutanol , Trichloroethylene , n-Butanol , 1,4-Dioxane , Toluene , Tetrachloroethylene , n-Butyl Acetate , Ethylbenzene , p-Xylene , Isoamyl Acetate , o-Xylene , n-Amyl Acetate , Cyclohexanol , Cyclohexanone , 2-Methylcyclohexanol , 2-Methylcyclohexanone , p-Dichlorobenzene , o-Dichlorobenzene , o-Cresol , m-Cresol
Applications
The work environment (2)
Column
ULBON HR-1701
Column Size
30m×0.53mm(5μm)
Column temp.
60°C→180°C(4°C/min)
Carrier gas
He,10ml/min
Detector temp.
200°C(FID)
Injection volume
1ml

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GC

Samples
Methanol , Ethanol , Acetone , IPA , n-Propanol , Ethyl Acetate , MEK , Chloroform , Benzene , n-Butanol , Toluene , MIBK , Isobutyl Acetate , n-Butyl Acetate , Ethylbenzene , m-Xylene , o-Xylene , Cellosolve Acetate
Applications
Solvents (2)
Column
ULBON HR-1701
Column Size
25m×0.32mm(0.5μm)
Column temp.
40°C→90°C(2°C/min)
Carrier gas
He,0.83ml/min
Detector temp.
200°C(FID)
Injection volume
1μl

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GC

Samples
Solvents (4)
Applications
Solvents (4)
Column
ULBON HR-1701
Column Size
50m×0.25mm(0.5μm)
Column temp.
60°C→180°C(4°C/min)
Carrier gas
He,1.4ml/min
Detector temp.
200°C(FID)
Injection volume
1μl

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GC

Samples
Acetaldehyde , Ethyl Acetate , Ethanol , 1-Propanol , 3-Pentanol , 2-Methyl-1-Butanol , 3-Methyl-1-Butanol
Applications
Scotch whisky
Column
ULBON HR-20M
Column Size
50m×0.32mm(1.0μm)
Column temp.
60°C→240°C(5°C/min)
Carrier gas
He,4.0ml/min
Detector temp.
250°C(FID)
Injection volume
0.6μl

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GC

Samples
n-Hexane , Ethyl Ether , Acetone , Methyl Acetate , trans-1,2-Dichloroethylene , Methanol , Isopropyl Acetate , Isopropanol , Dichloromethane , n-Propyl Acetate , cis-1,2-Dichloroethylene , Methyl Isobutyl Ketone , Chloroform , Toluene , 1,4-Dioxane , Isobutanol , Isoamyl Acetate , Ethylbenzene , p-Xylene , m-Xylene , Methyl Cellosolve , o-Xylene , Ethyl Cellosolve , Styrene , Cellosolve Acetate , N,N-Dimethylformamide , 4-Methylcyclohexanone , Butyl Cellosolve , cis-4-Methylcyclohexanol , m-Dichlorobenzene , p-Dichlorobenzene , trans-4-Methylcyclohexanol , o-Dichlorobenzene , o-Cresol , p-Cresol , m-Cresol
Applications
Solvents (6)
Column
ULBON HR-20M
Column Size
50m×0.25mm(0.5μm)
Column temp.
60°C→240°C(3°C/min)
Carrier gas
He,1.3ml/min
Detector temp.
250°C(FID)
Injection volume
1μl

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GC

Samples
Methanol , Acetone , Dichloromethane , trans-1,2-Dichloroethylene , n-Hexane , Ethyl Acetate , Tetrahydrofuran , 1,1,1-Trichloroethane , Carbon Tetrachloride , Trichloroethylene , Methyl Isobutyl Ketone , Toluene , Methyl Butyl Ketone , Tetrachloroethylene , Chlorobenzene , Ethylbenzene , p-Xylene , Styrene , 1,1,2,2-Tetrachloroethane , 2-Methylcyclohexanone , 4-Methylcyclohexanone , m-Dichlorobenzene , p-Dichlorobenzene , o-Cresol , p-Cresol
Applications
The work environment (1)
Column
ULBON HR-52
Column Size
30m×0.53mm(5μm)
Column temp.
60°C→130°C(3°C/min)
Carrier gas
He,8.0ml/min
Detector temp.
150°C(FID)
Injection volume
1ml

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GC

Samples
Methanol , Ethanol , Acetone , n-Propanol , n-Hexane , Ethyl Acetate , Chloroform , Benzene , MIBK , Toluene , Isobutyl Acetate , n-Butyl Acetate , Ethylbenzene , m-Xylene , o-Xylene , Cellosolve Acetate
Applications
Solvents (1)
Column
ULBON HR-52
Column Size
25m×0.32mm(0.5μm)
Column temp.
40°C→90°C(2°C/min)
Carrier gas
He,0.83ml/min
Detector temp.
200°C(FID)
Injection volume
1μl

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GC

Samples
Methanol , Acetone , Dichloromethane , trans-1,2-Dichloroethylene , n-Hexane , Ethyl Acetate , Tetrahydrofuran , 1,1,1-Trichloroethane , Carbon Tetrachloride , Trichloroethylene , 1,4-Dioxane , Methyl Isobutyl Ketone , Toluene , Methyl n-Butyl Ketone , n-Butyl Acetate , Tetrachloroethylene , Chlorobenzene , Ethylbenzene , p-Xylene , Styrene , o-Xylene , Butyl Cellosolve , 1,1,2,2-Tetrachloroethane , 3-Methylcyclohexanol(cis, trans) , 2-Methylcyclohexanone , 4-Methylcyclohexanone , m-Dichlorobenzene , p-Dichlorobenzene , o-Dichlorobenzene , o-Cresol , p-Cresol
Applications
Solvents (3)
Column
ULBON HR-52
Column Size
50m×0.25mm(0.5μm)
Column temp.
60°C→130°C(3°C/min)
Carrier gas
He,1.2ml/min
Detector temp.
200°C(FID)
Injection volume
1μl

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GC

Samples
α-Pinene , β-Pinene , Limonene , Linalool , Linalyl Acetate , Benzyl Acetate , Phenethyl Alcohol
Applications
perfume (1)
Column
ULBON HR-Thermon-600T
Column Size
50m×0.25mm
Column temp.
70°C→230°C(4°C/min)
Carrier gas
He,1.1ml/min
Detector temp.
250°C(FID)

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GC

Samples
β-Pinene , Limonene , Linalool , Linalyl Acetate , Benzyl Acetate , α-Ionene , Phenethyl Alcohol , Lauryl Alcohol , Eugenol , Diethyl Phthalate , Vanillin , Benzyl Salicylate
Applications
perfume (2)
Column
ULBON HR-Thermon-600T
Column Size
50m×0.25mm
Column temp.
70°C→230°C(4°C/min)
Carrier gas
He,1.1ml/min
Detector temp.
250°C(FID)

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GC

Samples
1,8-Cineole , β-Phenethyl Alcohol , Benzyl Acetate
Applications
Analysis of the fragrance of a flower using NeedlEx (for organic solvent) 1
Column
ULBON HR-1
Column Size
0.32mmI.D. × 30m (0.25um)
Column temp.
50°C→200°C(5°C/min)
Carrier gas
He,2.4ml/min
Detector temp.
250°C(FID)
Injection volume
-

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GC

Samples
Mixture of 13 organic solvents
Applications
Measurement of organic solvents using Shinwasorb -1-
Column
PEG1500 12.5% Shinwasorb-U 40/60
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
70℃
Carrier gas
40 mL/min N₂
Injection port temp.
200℃
Detector temp.
200℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Mixture of 22 organic solvents
Applications
Measurement of organic solvents using Shinwasorb -2-
Column
PEG1500 12.5% Shinwasorb-U 40/60
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
60~120℃ (4℃/min)
Carrier gas
40 mL/min N₂
Injection port temp.
200℃
Detector temp.
200℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Fragrance
Applications
Measurements of fragrance using Shinwasorb
Column
Thermon-3000 5% Shinwasorb-S 80/100
Column Size
2.1 m x 3.2 mm I.D. Glass
Column temp.
80~260℃(6℃/min)
Carrier gas
50 mL/min N₂
Injection port temp.
280℃
Detector temp.
280℃
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Ethyl acetate , di-n-butyl phthalate , Teprenone (mono-cis isomer) , Teprenone (all-trans isomer) , ,
Applications
Analysis of teprenone using Shinwasorb -1-
Column
FFAP 5% Shinwasorb-U 80/100
Column Size
2.1m×3.2mm glass
Column temp.
235°C
Carrier gas
47 mL/min N2
Injection port temp.
270°C
Detector temp.
270°C
Detector
FID
Injection volume
2.0 μL

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GC

Samples
Ethyl acetate , di-n-butyl phthalate , Teprenone (mono-cis isomer) , Teprenone (all-trans isomer) , ,
Applications
Analysis of teprenone using Shinwasorb -2-
Column
FFAP 5% Shinwasorb-U 80/100
Column Size
2.1m×3.2mm glass
Column temp.
235°C
Carrier gas
47 mL/min N2
Injection port temp.
270°C
Detector temp.
270°C
Detector
FID
Injection volume
2.0 µL

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GC

Samples
ethyl acetate
Applications
Analysis of sultamicillin tosilate hydrate using Sunpak-H
Column
Sunpak-H 80/100
Column Size
1.1 m x 3.2 mm I.D. Glass
Column temp.
130℃
Carrier gas
34 mL/min N2
Injection port temp.
200℃
Detector temp.
200℃  
Detector
FID
Injection volume
1.0 μL

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GC

Samples
ethyl acetate
Applications
Analysis of sultamicillin tosilate hydrate using Sunpak-H
Column
Sunpak-H 80/100
Column Size
1.1 m x 3.2 mm I.D. Glass
Column temp.
130℃
Carrier gas
34 mL/min N2
Injection port temp.
200℃
Detector temp.
200℃  
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Ethyl acetate , Caffeine , o-Toluene sulfonamide
Applications
Analysis of saccharin using Shinwasorb
Column
DEGS 1.5% Shinwasorb-S 60/80
Column Size
1.0 m x 3.0 mm I.D. Glass
Column temp.
210°C
Carrier gas
N2,55ml/min
Injection port temp.
225°C
Detector temp.
250°C
Detector
FID

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GC

Samples
Cyclohexane , Ethyl acetate , 2-propanol ,
Applications
Analysis of lenampicillin hydrochloride using Shinwasorb
Column
Quadrol 5% Shinwasorb-S 60/80
Column Size
3.1 m x 3.2 mm I.D. Glass
Column temp.
100℃
Carrier gas
70 mL/min N₂ (Adjust so that the retention time of cyclohexane is about 1 minute.)
Injection port temp.
160°C
Detector temp.
160°C
Detector
FID
Injection volume
4.0 μL

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GC

Samples
Isoflurane , Ethyl acetate
Applications
Analysis of isoflurane using Shinwasorb
Column
Igepal CO-880+Ucon LB-550X 5+7.5% Shinwasorb-S 100/120
Column Size
3.5 m x 3.0 mm I.D. Stainless steel
Column temp.
80℃
Carrier gas
37 mL/min N2 (Adjust so that the retention time of isoflurane is about 7 minutes.)
Injection port temp.
200°C
Detector temp.
200°C
Detector
FID
Injection volume
2.0 μL

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GC

Samples
Acetone , Ethyl acetate
Applications
Analysis of piperacillin hydrate using Sunpak-H ~(4) Residual solvents~
Column
Sunpak-H 80/100
Column Size
1.1m x 3.2 mm I.D. Glass
Column temp.
145℃
Carrier gas
33 mL/min N2 (Adjust so that the retention time of ethyl acetate is about 4 minutes.)
Injection port temp.
200°C
Detector temp.
200°C
Detector
FID
Injection volume
2.0 μL

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GC

Samples
Organic solvents
Applications
Analysis of organic solvents using Sunpak-A -1-
Column
Sunpak-A 50/80
Column Size
2.0 m x 3.0 mm I.D. Glass
Column temp.
150℃ ~ 220℃ (3 min hold) program rate 4℃/min
Carrier gas
50 mL/min N₂
Injection port temp.
250°C
Detector temp.
250°C
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Organic solvents
Applications
Analysis of organic solvents using Sunpak-A -2-
Column
Sunpak-A 50/80
Column Size
2.0 m x 3.0 mm I.D. Glass
Column temp.
150℃ ~ 220℃ (3 min hold) program rate 4℃/min
Carrier gas
50 mL/min N₂
Injection port temp.
250°C
Detector temp.
250°C
Detector
FID
Injection volume
1.0 μL

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GC

Samples
Diethyl ether , n-Hexane , Methanol , Methyl acetate , 2-Propanol , Ethyl acetate , Tetrahydrofuran , 2-Butanol , iso-Butanol , Toluene , n-Butyl acetate , Methyl n-butyl ketone , iso-Amyl alcohol , Ethylbenzene , m-Xylene , p-Xylene , o-Xylene , Styrene monomer ,
Applications
Measurement of organic solvents using SBS-120
Column
SBS-120 12% Shincarbon-A2 80/100
Column Size
3.1 m x 3.2 mm I.D. Glass
Column temp.
90℃
Carrier gas
40 mL/min N₂
Injection port temp.
230℃
Detector temp.
230℃
Detector
FID
Injection volume
1.0 μL

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LC

Samples
Methylphenidate
Applications
The central neuron stimulant
Column
ULTRON ES-CD
Column Size
150 mm L × 6.0 mm I.D.
Mobile phase
20 mM KH2PO4 (pH 6.0)/CH3CN = 90/10
Frow rate
1.2 mL/min
Column temp.
25°C

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LC

Samples
Mepenzolate bromide
Applications
Anticholinergic agent
Column
ULTRON ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 (pH 4.6)
Frow rate
1.0 mL/min
Column temp.
25°C

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LC

Samples
Vitamin A , Vitamin D2 , Vitamin D3 , Vitamin E , Tocopherol acetate
Applications
Fat-soluble vitamin
Column
STR ODS-II
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
CH3CN
Frow rate
1.0 mL/min
Column temp.
40°C

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LC

Samples
Montelukast sodium
Applications
Analysis of Montelukast sodium
Column
ULTRON ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
20 mM KH2PO4 + H3PO4 (pH 3.0)/CH3OH = 60/40
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
2.0 µL
Diluent
methanol

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LC

Samples
Clopidogrel Related Compound A , Clopidogrel Related Compound B , Clopidogrel Related Compound C , Clopidogrel bisulfate
Applications
Analyses of Clopidogrel Related Compounds in ULTRON ES-OVM series.(Faster analyses with 3µm particles)
Column
ULTRON ES-OVM
Column Size
(1)150 mm L × 4.6 mm I.D. (2)100 mm L × 3.0 mm I.D.
Mobile phase
10 mM KH2PO4/CH3CN = 75/25
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
(1)10.0 µL (2)3.0 µL

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Graph

LC

Samples
Clopidogrel Related Compound A , Clopidogrel Related Compound B , Clopidogrel Related Compound C , Clopidogrel bisulfate
Applications
Analysis of Clopidogrel Related Compounds
Column
ULTRON ES-OVM
Column Size
150 mm L × 4.6 mm I.D.
Mobile phase
10 mM KH2PO4/CH3CN = 75/25
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
10.0 µL

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LC

Samples
Clopidogrel Related Compound A , Clopidogrel Related Compound B , Clopidogrel Related Compound C , Clopidogrel bisulfate
Applications
Analysis of Clopidogrel Related Compounds
Column
ULTRON ES-OVM
Column Size
100 mm L × 3.0 mm I.D.
Mobile phase
10 mM KH2PO4/CH3CN = 75/25
Frow rate
1.0 mL/min
Column temp.
25°C
Injection volume
3.0 µL

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